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Beilstein J. Org. Chem. 2021, 17, 1041–1047, doi:10.3762/bjoc.17.83
Graphical Abstract
Scheme 1: AB-mediated reductions of nitrostyrenes 3a–h.
Scheme 2: AB-mediated reductions of nitrostyrenes 1, 3a, and 3c using DESs B and D.
Scheme 3: AB-mediated reductions of nitroalkenes 5a–f.
Scheme 4: Recovery and recycling experiments in the AB-mediated reduction of nitrostyrene 3h to afford nitroa...
Beilstein J. Org. Chem. 2016, 12, 2620–2626, doi:10.3762/bjoc.12.258
Scheme 1: L-Proline-promoted stereoselective aldol reaction in DES.
Figure 1: Experimental set-up I: test tube (d = 0.5 cm); flow 1 mL/min; DES (1.5 mL); L-proline/DES = 130 mg/...
Scheme 2: Aldol reaction under continuous flow conditions in DESs.
Beilstein J. Org. Chem. 2016, 12, 2614–2619, doi:10.3762/bjoc.12.257
Scheme 1: Continuous flow reduction of 4-nitrobenzophenone using a 0.5 mL PTFE flow reactor.
Scheme 2: Continuous flow reduction of aromatic nitro compounds.
Scheme 3: Continuous-flow reduction of aliphatic nitro compounds.
Scheme 4: Synthesis of 2-(4’-chlrophenyl)aniline (4) with a 5 mL flow reactor.
Scheme 5: Synthesis of intermediate 6, a direct precursor of the drug baclofen.
Scheme 6: Continuous-flow reduction of 1a and in-line extraction.